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Iskalni niz: "polno besedilo" AND "organizacija" (Inštitut za kovinske materiale in tehnologije) .

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Ultra-high strenght TWIP steel with high chromium content
Pavel Podaný, Tomáš Studecký, Tomas Gregor, Radek Prochazka, Aleksandra Kocijan, 2023, izvirni znanstveni članek

Povzetek: A new ultra-high strength steel with a fully austenitic microstructure and twinning-induced plasticity (TWIP) effect has been developed. TWIP effect gives this steel a good combination of high strength of over 1000 MPa and ductility of over 35%. This new steel has a high chromium content, which increases its corrosion resistance. By combining cold rolling and annealing, the steel has achieved a very fine austenitic microstructure with an average grain diameter of 2.85 µm. This steel could be used for structural applications or components that need to withstand high levels of stress, deformation and corrosion environment.
Ključne besede: TWIP steels, corrosion resistance, microstructure, tensile strength, plasticity
Objavljeno v DiRROS: 31.01.2024; Ogledov: 201; Prenosov: 81
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84.
Improving the surface properties of additive-manufactured Inconel 625 by plasma nitriding
Danijela Anica Skobir Balantič, Črtomir Donik, Bojan Podgornik, Aleksandra Kocijan, Matjaž Godec, 2023, izvirni znanstveni članek

Povzetek: As a surface-hardening technique, plasma nitriding is a common procedure for improving the properties of conventional Ni-based alloys. The diffusion of nitrogen hardens a layer on the surface of the alloy, leading to better wear resistance and a higher coefficient of friction, as well as a higher surface hardness. This study reports the effect of plasma nitriding on additive-manufactured (AM) Inconel 625 (IN625) compared to its conventional manufactured and nitrided counterparts. The samples produced with the laser powder-bed fusion (LPBF) process were subsequently plasma nitrided in the as-built condition, stress-relief annealed at 870 °C and solution treated at 1050 °C. The plasma nitridings were carried out at 430 °C and 500 °C for 15 h. The growth kinetics of the nitride layer of the AM samples depends on the prior heat treatments and is faster in the as-built state due to the specific cellular structure. The lower nitriding temperature leads to the formation of expanded austenite in the nitride layer, while at the higher nitriding temperature, the expanded austenite decomposes and CrN precipitation occurs. The XRD and SEM analyses confirmed the presence of two layers: the surface layer and the diffusion layer beneath. The lower nitriding temperature caused the formation of expanded austenite or a combination of expanded austenite and CrN. The higher nitriding temperature led to the decomposition of the expanded austenite and to the formation/precipitation of CrN. The higher nitriding temperature also decreased the corrosion resistance slightly due to the increased number of precipitated Cr-nitrides. On the other hand, the wear resistance was significantly improved after plasma nitriding and was much less influenced by the nitriding temperature.
Ključne besede: additive manufacturing, powder-bed fusion, plasma nitriding, expanded austenite, wear and corrosion resistance, Ni-based alloy
Objavljeno v DiRROS: 31.01.2024; Ogledov: 187; Prenosov: 79
.pdf Celotno besedilo (7,98 MB)
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85.
Relevance of inter-particle interaction in directed energy deposition powder stream
Tijan Mede, Matjaž Godec, 2024, izvirni znanstveni članek

Povzetek: Blown powder dynamics is one of the aspects of Directed Energy Deposition (DED) with a major influence on deposition quality and potential for improvement in simulation. Most currently employed computational models discard powder grain collisions as negligible, although little explicit evidence for that claim exists. A Discrete Element Method approach is thus employed in the present work to simulate the actual number of grain collisions in a powder stream of a commercial discrete coaxial nozzle and how that number varies with the key processing parameters. While the number of powder grain collisions is found to in fact be negligible at one side of the usable parameter spectrum, the opposite side results in as many as 84% of all the powder grains being involved in inter-granular collisions with an average rebound angle of 14◦, challenging the established hypothesis of the negligibility of this phenomena.
Ključne besede: DED, powder stream, grain collisions, DEM
Objavljeno v DiRROS: 31.01.2024; Ogledov: 113; Prenosov: 65
.pdf Celotno besedilo (1,65 MB)
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86.
High-temperature oxidation of boiler steels at 650 °C
Jaka Burja, Barbara Šetina, Borut Žužek, Tilen Balaško, 2023, izvirni znanstveni članek

Povzetek: This study presents a comprehensive investigation of the formation, composition and behaviour of oxide layers during the high-temperature oxidation of four different steel alloys (16Mo3, 13Cr, T24 and P91) at a uniform temperature of 650 °C. The study is aimed at assessing the oxidation damage due to short-term overheating. The research combines CALPHAD (CALculation of PHAse Diagrams) calculations, thermogravimetric analysis (TGA) and advanced microscopy techniques, in- cluding scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD), to elucidate the complex mechanisms controlling oxidation kinetics and oxide layer development. CALPHAD calculations were used to determine the thermodynamically stable phases for each steel type at 650 ◦C and different oxygen activities. The results showed different phase compositions, highlighting the importance of the chromium content in steel for the formation of oxide layers. The different oxidation kinetics and oxide layer compositions are presented and associated with the increased risk of material degradation due to overheating. These results have significant implications for industrial applications, mainly the susceptibility to oxidation of low-alloyed steels like 16Mo3 and 13 Cr and contribute to a deeper understanding of oxidation processes in steels.
Ključne besede: high-temperature oxidation, thermogravimetric analysis, kinetics, CALPHAD, boiler steels, SEM, EBSD
Objavljeno v DiRROS: 26.01.2024; Ogledov: 236; Prenosov: 113
.pdf Celotno besedilo (12,99 MB)
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87.
Morphological characteristics of young and old murine hematopoietic stem cell niches, as modeled in vitro
Mojca Justin, Ema Rogac Randl, Veno Kononenko, Matej Hočevar, Damjana Drobne, Primož Rožman, 2023, izvirni znanstveni članek

Povzetek: The hematopoietic stem cell (HSC) niche undergoes detrimental changes with age. The molecular differences between young and old niches are well studied and understood; however, young and old niches have not yet been extensively characterized in terms of morphology. In the present work, a 2D stromal model of young and old HSC niches isolated from bone marrow was investigated using light and scanning electron microscopy (SEM) to characterize cell density after one, two, or three weeks of culturing, cell shape, and cell surface morphological features. Our work is aimed at identifying morphological differences between young and old niche cells that could be used to discriminate between their respective murine HSC niches. The results show several age- specific morphological characteristics. The old niches differ from the young ones in terms of lower cell proliferating capacity, increased cell size with a flattened appearance, increased number of adipocytes, and the presence of tunneling nanotubes. In addition, proliferating cell clusters are present in the young niches but not in the old niches. Together, these characteristics could be used as a relatively simple and reliable tool to discriminate between young and old murine HSC niches and as a complementary approach to imaging with specific cellular markers.
Ključne besede: bone marrow, hematoopetic stem cell niche, aging, adipocytes, scanning electron microscopy
Objavljeno v DiRROS: 26.01.2024; Ogledov: 213; Prenosov: 106
.pdf Celotno besedilo (2,47 MB)
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