1. Effect of deep cryogenic treatment on corrosion properties of various high-speed steelsJure Voglar, Živa Novak, Patricia Jovičević Klug, Bojan Podgornik, Tadeja Kosec, 2021, izvirni znanstveni članek Povzetek: The aim of the study was to evaluate the corrosion properties of three different grades of high-speed steel following a heat treatment procedure involving deep cryogenic treatment after quenching and to investigate how these properties are connected to the microstructure and hard- ness of the material. The hardness of steels was measured, and microstructural properties were determined through observation of the metallographically prepared steels using scanning electron microscopy. These studies were complemented corrosion evaluation by the use of corrosion potential measurement and linear polarization measurement of steels in a sodium tetraborate buffer at pH 10. The results showed that the deep cryogenic procedure of high-speed steel changed the microstructure and consequently affected the hardness of the investigated steels to different extents, depending on their chemical composition. Corrosion studies have confirmed that some high-speed steels have improved corrosion properties after deep cryogenic treatment. The most important improvement in corrosion resistance was observed for deep cryogenically treated high-speed steel EN 1.3395 (M3:2) by 31% when hardened to high hardness values and by 116% under lower hardness conditions. The test procedure for differentiating corrosion properties of differently heat-treated tool steels was established alongside the investigation.
Ključne besede: deep cryogenic treatment, corrosion, microstructure, hardness
Objavljeno v DiRROS: 01.08.2023; Ogledov: 83; Prenosov: 37
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2. Differences between 3-D printed and traditionally milled CoCr dental alloy from casted block in oral environmentMirjam Bajt Leban, Matej Kurnik, Igor Kopač, Matic Klug Jovičević, Bojan Podgornik, Tadeja Kosec, 2023, izvirni znanstveni članek Povzetek: The aim of this study was to compare corrosion resistance and ion release in CoCr dental alloys with identical chemical compositions produced using different technologies (SLM – selective laser melting and milling from cast blocks) and heat treatment (SLM parts only). The corrosion properties were tested in artificial saliva, artificial saliva with fluoride ions, and artificial saliva with added lactic acid to simulate inflammations. The study included electrochemical tests, microstructural investigation and ion release tests in the three different environments for a total of 42 days. The best performance of CoCr as a result of potentiodynamic polarization was observed in the artificial saliva with added lactic acid, which is in contradiction with the highest ion release measured from all the materials tested and electrochemical impedance spectroscopy that showed a deterioration of the passive layer in an acidic environment. Microstructural investigation revealed that different phases precipitated by heat treatment trigger increased release of Mo and W ions. The printing method does not raise critically ion release from CoCr alloy, while the state of the surface greatly impacts the extent of the ion release. This study demonstrates the importance of an interdisciplinary approach to the study of corrosion and biocompatibility in dental alloys.
Ključne besede: CoCr dental alloy, selective laser melting, corrosion, ion release, artificial saliva
Objavljeno v DiRROS: 29.05.2023; Ogledov: 103; Prenosov: 73
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3. Influence of the deep cryogenic treatment on AISI 52100 and AISI D3 steelʼs corrosion resistancePatricia Jovičević Klug, Tjaša Kranjec, Matic Klug Jovičević, Tadeja Kosec, Bojan Podgornik, 2021, izvirni znanstveni članek Povzetek: The effect of deep cryogenic treatment (DCT) on corrosion resistance of steels AISI 52100 and AISI D3 is investigated and compared with conventional heat-treated counterparts. DCTʼs influence on microstructural changes is subsequently correlated to the corrosion resistance. DCT is confirmed to reduce the formation of corrosion products on steelsʼ surface, retard the corrosion products development and propagation. DCT reduces surface cracking, which is considered to be related to modified residual stress state of the material. DCTʼs influence on each steel results from the altered microstructure and alloying element concentration that depends on steel matrix and type. This study presents DCT as an effective method for corrosion resistance alteration of steels.
Ključne besede: steel, deep cryogenic treatment, corrosion, Raman, open access
Objavljeno v DiRROS: 19.05.2023; Ogledov: 101; Prenosov: 70
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4. Effect of laser texturing pattern on Ti6Al4Vtribocorrosion in a physiological solutionMarjetka Conradi, Tadeja Kosec, Bojan Podgornik, Aleksandra Kocijan, Janez Kovač, Damjan Klobčar, 2022, izvirni znanstveni članek Povzetek: Laser texturing is a process that alters a material’s surface properties by modifying its morphology, which can improve properties like adherence, wettability, thermal and electrical conductivity and friction. Here, the effect of laser texturing was studied on an alpha-beta titanium alloy (Ti6Al4V) biomedical material. Two types of patterned surfaces, cross-hatch with varying scan-line separations, Dx = 100, 180 and 280 μm and dimples of 200 μm size, were prepared on the surface of alpha-beta titanium alloy by laser technology. Prepared samples were characterised for their surface properties, such as corrosion, wear-induced corrosion, friction and wettability. Electrochemical and tribocorrosion properties in a physiological solution were studied on the samples with different texture densities of cross-hatch pattern and dimples and compared to the as-received alpha-beta titanium alloy surface. Corrosion rate decreased for laser-textured samples, especially for cross-hatch texture (down to 1 μm/year for Dx = 180 μm) when compared to the as-received alpha-beta titanium alloy surface due to the changed laser-induced surface film and wetting properties. Friction coefficient slightly decreased for all laser-textured surfaces, most noticeably for cross-hatch patterns, from 0.38 (as-received) down to 0.34 (Dx = 180 and 280 μm). The main contribution to total wear in physiological solution increased due to the mechanical wear, which is governed by the removal of the surface oxide layer induced by laser texturing.
Ključne besede: TiAIV, laser texturing, tribocorrosion, open access
Objavljeno v DiRROS: 17.05.2023; Ogledov: 89; Prenosov: 34
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7. Revealing the Pb whisker growth mechanism from Al-alloy surface and morphological dependency on material stress and growth environmentMatic Klug Jovičević, Tim Verbovšek, Patricia Jovičević Klug, Barbara Šetina, Bojan Ambrožič, Goran Dražić, Bojan Podgornik, 2022, izvirni znanstveni članek Ključne besede: aluminum alloy, metallic whiskers, residual stress, crystal growth, oxidation
Objavljeno v DiRROS: 06.05.2022; Ogledov: 372; Prenosov: 120
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8. Water versus oil lubrication of laser-textured Ti6Al4V alloy upon addition of MoS2 nanotubes for green tribologyMarjetka Conradi, Bojan Podgornik, Aleksandra Kocijan, Maja Remškar, Damjan Klobčar, 2022, izvirni znanstveni članek Ključne besede: green tribology, surface texturing, MoS2 nanotubes, lubrication, Ti6Al4V alloy
Objavljeno v DiRROS: 06.05.2022; Ogledov: 306; Prenosov: 96
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10. The influence of the plasma-nitriding temperature on the microstructure evolution and surface properties of additive-manufactured 18Ni300 maraging steelMatjaž Godec, Francisco Ruiz-Zepeda, Bojan Podgornik, Črtomir Donik, Aleksandra Kocijan, Danijela Anica Skobir Balantič, 2022, izvirni znanstveni članek Ključne besede: maraging steel, powder bed fusion, plasma nitriding, microstructure, wear resistance, corrosion resistance
Objavljeno v DiRROS: 06.05.2022; Ogledov: 348; Prenosov: 107
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