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Iskalni niz: "ključne besede" (pressureless spark plasma sintering) .

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1.
Rapid radiation sintering of additively manufactured large-sized alumina tetrahedrons
Aljaž Iveković, Miha Križaj, Andraž Kocjan, 2026, izvirni znanstveni članek

Povzetek: Rapid radiation techniques, such as pressureless spark plasma sintering (pSPS) and ultra-fast high-temperature sintering (UHS), have proven effective in achieving rapid densification of ceramics, including additively manufactured components. However, sintered component sizes tend to be small, disk-shaped or having thin-strutted geometries. Here, fused filament fabrication (FFF) of a commercial filament was used for manufacturing complex-shaped and large-sized alumina tetrahedra with edge thickness of 5 mm, varying the edge size (15‒40 mm). The aim was to investigate the effect of heating rate (33‒300°C/min) and tetrahedron size on the pSPS outcome. The pSPS reductive environment discoloured the tetrahedra, but were all successfully rapidly sintered to full density irrespective of their size and heating rate employed. The evolved thermal gradient contributed to differential, anisotropic densification related shrinkage, microstructure and mechanical properties specific to tetrahedra` edge position, i.e., core versus shell and base versus lateral, also triggering cracking of the largest tetrahedra.
Ključne besede: additive manufacturing, fused filament fabrication, pressureless spark plasma sintering
Objavljeno v DiRROS: 15.06.2026; Ogledov: 106; Prenosov: 77
.pdf Celotno besedilo (7,97 MB)
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2.
The role of carbon presence on the strontium hexaferrite phase decomposition during pressureless spark plasma sintering (pSPS)
Aleksander Učakar, Andraž Kocjan, Blaž Belec, Janez Košir, Tanja Kallio, Marjeta Maček, Bor Arah, Petra Jenuš, 2025, izvirni znanstveni članek

Povzetek: The phase composition and microstructure of Sr-hexaferrite (SFO) ceramics govern the hard magnetic properties. Here, pressureless spark plasma sintering (pSPS) technique was employed for the rapid consolidation (500°C/min) of SFO in a radiating graphite crucible under vacuum and, thus, reductive conditions. A numerical model depicting the temperature profile within the heating crucible was constructed to understand the temperature evolution within the samples. The combination pSPS sintering environment (graphite heating crucible under vacuum) promoted phase decomposition to Sr-enriched and depleted phases of various morphological variations, leading to reduction of hard magnetic properties. Notably, certain newly formed phases exhibited lower melting points, inducing a shift in the sintering mechanism from solid-state sintering to a partial liquid-phase sintering mechanism.
Ključne besede: pressureless spark plasma sintering, electronic ceramics, numerical simulations
Objavljeno v DiRROS: 03.09.2025; Ogledov: 805; Prenosov: 795
.pdf Celotno besedilo (11,24 MB)
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