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Abstract: Selective laser melting (SLM) is an additive manufacturing process, forming the desired geometry by selective layer fusion of powder material. Unlike conventional manufacturing processes, highly complex parts can be designed and manufactured with high accuracy and little post processing. Currently, different types of steel, aluminium, titanium and nickel-based alloys have been successfully processed; however, high strength aluminium alloy EN AW 7075 has not been processed with satisfying quality. The main focus of the investigation is to develop a new alloy which is more suitable for the SLM process for the wide used aluminium alloy EN AW 7075. But before that, gas-atomized powder material was characterized in terms of statistical distribution. A wide range of process parameters and different pre-heating temperatures were selected to optimize the process in terms of optimum volume density and reducing the effect of hot cracking. However, all laser-melted parts exhibited hot cracks which typically appear in aluminium alloy EN AW 7075.
Keywords: EN AW 7075, aluminium alloy, hot cracks, relative density, selective laser melting (SLM)
Published in DiRROS: 22.04.2024; Views: 90; Downloads: 0

Abstract: In this paper we present the main developments in Oka theory since the publication of my book "Stein Manifolds and Holomorphic Mappings (The Homotopy Principle in Complex Analysis)", 2nd ed., Springer, 2017. We also give several new results, examples and constructions of Oka domains in Euclidean and projective spaces. Furthermore, we show that for $n > 1$ the fibre $\mathbb C^n$ in a Stein family can degenerate to a non-Oka fibre, thereby answering a question of Takeo Ohsawa. Several open problems are discussed.
Keywords: Oka manifold, Oka map, Stein manifold, elliptic manifold, algebraically subelliptic manifold, Calabi–Yau manifold, density property
Published in DiRROS: 14.03.2024; Views: 418; Downloads: 454
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Abstract: Let $X$ be a Stein manifold of complex dimension $n \ge 1$ endowed with a Riemannian metric ${\mathfrak g}$. We show that for every integer $k$ with $\left[\frac{n}{2}\right] \le k \le n-1$ there is a nonsingular holomorphic foliation of dimension $k$ on $X$ all of whose leaves are topologically closed and ${\mathfrak g}$-complete. The same is true if $1\le k \left[\frac{n}{2}\right]$ provided that there is a complex vector bundle epimorphism $TX\to X \times \mathbb{C}^{n-k}$. We also show that if $\mathcal{F}$ is a proper holomorphic foliation on $\mathbb{C}^n$ $(n > 1)$ then for any Riemannian metric ${\mathfrak g}$ on $\mathbb{C}^n$ there is a holomorphic automorphism $\Phi$ of $\mathbb{C}^n$ such that the image foliation $\Phi_*\mathcal{F}$ is ${\mathfrak g}$-complete. The analogous result is obtained on every Stein manifold with Varolin's density property.
Keywords: Stein manifolds, complete holomorphic foliations, density property
Published in DiRROS: 19.02.2024; Views: 185; Downloads: 63
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Abstract: Our study presents a comprehensive approach for the selective oxidation of glucose to glucaric acid (GA) by heterogeneous catalysis. We have synthesized and characterized Au/ZrO2, AuCu/ZrO2 and AuPt/ZrO2 catalysts using X-ray diffraction (XRD), transmission electron microscopy (TEM), X-ray photoelectron spectroscopy (XPS), and oxygen pulse chemisorption (OPS) techniques. Combining experimental observations with in-depth density functional theory (DFT) studies, we found that bimetallic catalysts form alloys, which exhibit different characteristics than monometallic counterparts for the given reaction. We performed batch reactions, varying temperature and oxygen pressure, and used the data to construct a predictive microkinetic model. As it turned out, AuPt/ZrO2 showed the highest selectivity, yielding 32 % of GA at 100 °C and 30 barg O2. Our results provide valuable insights for the developing of efficient catalysts and point out the bottlenecks for the oxidation of glucose to GA.
Keywords: glucaric acid, glucose oxidation, catalyst characterization, density functional theory, microkinetic modelling
Published in DiRROS: 06.12.2023; Views: 224; Downloads: 134
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Abstract: We examined activation patterns of the gastrocnemius medialis (GM), gastrocnemius lateralis (GL), soleus (SO), and tibialis anterior (TA) muscles in eight older (58.4 ± 3.3 years) and seven young (23.1 ± 2.9 years) participants, before and after 14 days of horizontal bed rest. Visual feedback on the exerted muscle torque was provided to the participants. The discharge patterns of individual motor units (MUs) were studied in three repetitions of isometric plantar flexion at 30 and 60% of Maximum Voluntary Contraction (MVC), before, and 1 day after the 14-day bed rest, respectively. In the GL and GM muscles, the older participants demonstrated higher MU discharge rates than the young, regardless of the contraction level, both before and after the bed rest. In the TA and SO muscles, the differences between the older and young participants were less consistent. Detailed analysis revealed person-specific changes in the MU discharge rates after the bed rest. To quantify the coactivation patterns we calculated the correlation coefficients between the cumulative spike trains of identified MUs from each muscle, and measured the root mean square difference of the correlation coefficients between the trials of the same session (intra-session variability) and between different sessions (inter-session variability) in each participant (intra-person comparison) and across participants (inter-person comparison). In the intra-person comparison, the inter-session variability was higher than the intra-session variability, either before or after the bed rest. At 60% MVC torque, the young demonstrated higher inter-person variability of coactivation than the older participants, but this variability decreased significantly after the bed rest. In older participants, inter-person variability was consistently lower at 60% than at 30% MVC torque. In young participants, inter-person variability became lower at 60% than at 30% MVC torque only after the bed rest. Precaution is required when analyzing the MU discharge and coactivation patterns, as individual persons demonstrate individual adaptations to aging or bed rest.
Keywords: high density electromyography, muscle disuse, motor units, discharge rate, aging
Published in DiRROS: 05.09.2022; Views: 633; Downloads: 357
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