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Title:Effects of the temperature on the pore evolution during sintering of the belite-sulfoaluminate cement clinker using x-ray computed microtomography
Authors:ID Dolenec, Sabina (Author)
ID Korat, Lidija (Author)
ID Mrak, Maruša (Author)
ID Ipavec, Andrej (Author)
ID Žibret, Lea (Author)
Files:.pdf PDF - Presentation file, download (2,27 MB)
MD5: 336C4FB1CCCF272A2866C44DF1CF34D9
 
URL URL - Source URL, visit https://doi.org/10.17222/mit.2020.031
 
Language:Slovenian
Typology:1.01 - Original Scientific Article
Organization:Logo ZAG - Slovenian National Building and Civil Engineering Institute
Abstract:In this paper, the effects of the sintering temperature on the pore evolution of the belite-sulfoaluminate cement clinker were evaluated. Belite-sulfoaluminate cement clinker with a targeted composition of 65 w/% b-belite, 20 w/% calcium sulfoaluminate and 10 w/% ferrite was sintered at three different temperatures: 1200 °C, 1250 °C and 1300 °C. To quantitatively evaluate the pore evolution during sintering, a 3D microstructure reconstruction by micro-CT was used. From the data, the pore volume frac- tion and pore number were extracted and compared, and the pore size distribution with the sintering temperature was obtained as well. Additionally, the pore shape and distribution were displayed in 3D based on actual microstructure data. Clinker samples were also characterized by Hg-intrusion porosimetry and gas sorption. The changes in the pore evolution occurred to a larger extent when sintering at 1300 °C. Apart from a significant porosity decrease, pore coarsening was evident at this temperature, reducing their connectivity and shrinkage of the clinker. Simultaneously, the bulk and apparent densities increased with the temperature due to densification, while the BET surface area of the studied clinkers decreased, indicating the rounding of pores and particle coalescence with an increasing grain growth.
Keywords:klinker, belit-sulfoaluminat, razvoj por, sintranje
Publication status:Published
Publication version:Version of Record
Publication date:01.09.2020
Publisher:Inštitut za kovinske materiale in tehnologije
Year of publishing:2020
Number of pages:str. 705-713
Numbering:Letn. 54, št. 5
PID:20.500.12556/DiRROS-16458 New window
UDC:620.1/.2
ISSN on article:1580-2949
DOI:10.17222/mit.2020.031 New window
COBISS.SI-ID:33213699 New window
Copyright:© MATERIALI IN TEHNOLOGIJE
Note:Nasl. v angl. in slov., besedilo v angl.;
Publication date in DiRROS:04.08.2023
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Record is a part of a journal

Title:Materiali in tehnologije
Shortened title:Mater. tehnol.
Publisher:Inštitut za kovinske materiale in tehnologije
ISSN:1580-2949
COBISS.SI-ID:106193664 New window

Document is financed by a project

Funder:Other - Other funder or multiple funders
Project number:C3330-17-529035
Name:Raziskovalci- 2.0-ZAG-529035

Funder:ARRS - Slovenian Research Agency
Project number:P2-0273
Name:Gradbeni objekti in materiali

Licences

License:Other
Description:The journal MATERIALI IN TEHNOLOGIJE/MATERIALS AND TECHNOLOGY is an open access journal, this means its free availability on the public internet, permitting any users to read, download, copy, distribute, print, search, or link to the full texts of these articles, crawl them for indexing, pass them as data to software, or use them for any other non-commercial purposes, without financial, legal, or technical barriers other than those inseparable from gaining access to the internet itself. The only constraint is on reproduction, and the only role for copyright in this domain, should be to give authors control over the integrity of their work and the right to be properly acknowledged and cited.
Applies to:http://mit.imt.si/index-slo.html

Secondary language

Language:English
Title:Razvoj por med sintranjem belitno-sulfoaluminatnega cementnega klinkerja z rentgensko računalniško mikrotomografijo
Abstract:Prispevek obravnava vpliv temperature sintranja na razvoj por pri belitno-sulfoaluminatnem cementnem klinkerju. Klinker želeno sestavo faz 65 w/% b-belita, 20 w/% kalcijevega sulfoaluminata in 10 w/% ferita je bil sintran pri treh različnih temperaturah: 1200 °C, 1250 °C in 1300 °C. Z računalniško mikrotomografijo smo na podlagi 3D rekonstrukcije mikrostrukture kvantitativno ocenili razvoj por pri sintranju. Iz podatkov smo pridobili delež volumna por in število por ter tudi porazdelitev por. Poleg tega je bila v 3D prikazana tudi oblika in porazdelitev por. Vzorci klinkerja so bili okarakterizirani tudi živosrebrovo porozimetrijo in plinsko sorpcijo. Rezultati kažejo, da so se največje spremembe pri razvoju por zgodile pri sintranju na 1300 °C. Poleg občutnega zmanjšanja poroznosti je bilo pri tej temperaturi opaziti tudi večanje por, zmanjševanje povezanosti med njimi in krčenje klinkerja. Obenem sta se volumska in navidezna gostota s temperaturo povečali zaradi zgoščevanja, medtem ko se je specifična površina BET klinkerjev zmanjšala, kar kaže na zaobljevanje por in povečevanje zrn.
Keywords:clinker, belite-sulfoaluminate, pore evolution, sintering


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