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4. Characterisation of the microstructure and defects during the direct energy deposition of hybrid Ti6Al4V in a low-quality atmosphereSimon Malej, Črtomir Donik, Matej Balažic, Matija Bizjak, Marko Kač, Matjaž Godec, 2023, original scientific article Keywords: direct energy deposition, Ti6Al4V, protective atmosphere Published in DiRROS: 08.03.2024; Views: 277; Downloads: 137 Full text (3,66 MB) This document has many files! More... |
5. Mechanisms of premature fracture in modular neck stems made of CoCrMo/Ti6Al4V and Ti6Al4V/Ti6Al4V alloyDrago Dolinar, Miro Gorenšek, Klemen Avsec, Barbara Šetina, Matej Hočevar, Matjaž Godec, Borut Žužek, Mojca Debeljak, Monika Jenko, John T. Grant, Boštjan Kocjančič, 2023, original scientific article Abstract: In this paper, we present the mechanisms of premature fracture of modular neck stems in two case studies: (I) when the neck and stem are both made of the same Ti6Al4V alloy, and (II) when the neck and stem are made from two different alloys, CoCrMo and Ti6Al4V alloy. Our study integrates two orthopedic patients who have undergone primary uncemented THA for usual indications in two orthopedic centers (Community Health Centre and University Medical Centre). Both centers are part of the national public health care system. Both surgeries were performed by two skilled orthopedic surgeons with more than 10 years of experience in THA. The survivorship of the modular neck of cast CoCrMo alloy was 24 months. The survivorship of the modular neck from Ti6Al4V alloy was 84 months. Multivariate analyses were performed to assess the differences in the fretting, corrosion, and fatigue of the two prematurely failed modular neck stems: stereo light microscopy (SLM), scanning electron microscopy (SEM), X-ray energy-dispersive spectroscopy (EDS), and electron backscatter diffraction (EBSD). Patient demographic information, including sex, age, body mass index, survivorship of implants, and reason for the revision, was collected from medical records. We found that fretting and fatigue occurred on both neck-stem retrievals due to additional galvanic corrosion, but the CoCrMo/Ti6Al4V alloy system suffered more corrosion due to additional galvanic corrosion and fractured earlier than the Ti6Al4V/Ti6Al4V metal alloy system. Both metallic alloy systems used in this application are known to be highly corrosion-resistant, but the bio-tribo-corrosion processes need to be understood in detail and characterized so that appropriate improvements in design and materials can be made. Keywords: total hip arthroplasty, modular neck, Ti6Al4V alloy, CoCrMo alloy, corrosion Published in DiRROS: 07.02.2024; Views: 414; Downloads: 218 Full text (5,12 MB) This document has many files! More... |
6. Hybrid additive manufacturing of Ti6Al4V with powder-bed fusion and direct-energy depositionSimon Malej, Matjaž Godec, Črtomir Donik, Matej Balažic, René Zettler, Thomas Lienert, Laurent Pambaguian, 2023, original scientific article Keywords: hybrid additive manufacturing, Ti6Al4V, tensile properties, defects, microstructure, phase transformation Published in DiRROS: 02.02.2024; Views: 357; Downloads: 170 Full text (18,54 MB) This document has many files! More... |
7. The corrosion resistance of dental Ti6Al4V with differing microstructures in oral environmentsMirjam Bajt Leban, Tadeja Kosec, Matjaž Finšgar, 2023, original scientific article Abstract: The impact of the microstructural properties of a Ti6Al4V alloy on its electrochemical properties, as well as the effect of the α- and β-phases present within it, is still unclear. With the introduction of new, emerging technologies, such as selective laser melting and post heat treatments, the effect of the microstructure on an alloy's corrosion properties has become increasingly interesting from a scientific perspective. When these alloys are produced through different methods, despite an identical chemical composition they have diverse microstructures, and consequently display varying resistance to corrosion. In the present research study, Ti–6Al–4V alloy specimens produced by three different processes, leading to the formation of three different microstructures were investigated: heat treated specimen fabricated by selective laser melting, wrought and cast specimens. The impact of the microstructure of these alloys when immersed in artificial saliva was studied through the use of various electrochemical techniques, by microscopical examinations, and time-of-flight secondary ion mass spectrometry. Corrosion properties were investigated by the measurement of open circuit potential, linear polarization, and potentiodynamic curve measurements followed by microscopical examinations, and time-of-flight secondary ion mass spectrometry examination was conducted to reveal spatial distribution of alloying species on oxide film. It was found that the difference between specimens containing an α+β microstructure was small and not dependent on the aspect ratio of the β-phase, alloy grain size, and vanadium partitioning coefficient, but rather on the size, shape, and content of this phase. Keywords: Ti6Al4V, dental alloy, microstructure, corrosion resistance, heat treatment, ToF-SIMS Published in DiRROS: 26.10.2023; Views: 720; Downloads: 376 Full text (8,12 MB) This document has many files! More... |
8. Corrosion characterization and ion release in SLM-manufactured and wrought Ti6Al4V alloy in an oral environmentMirjam Bajt Leban, Tadeja Kosec, Matjaž Finšgar, 2022, original scientific article Abstract: As-produced and heat-treated TiAlV samples were prepared by selective laser melting and compared to wrought samples of identical chemical composition. Microstructural, corrosion, and spectroscopic studies of additively manufactured samples in artificial saliva at 37 °C, with NaF and at pH 2.3 were as a novelty combined with metal ion release during 42 days immersion. In artificial saliva higher amount of ions was released on SLM specimen when compared to wrought alloy. The total amount of ions released from SLM specimen in AS containing NaF was 10-times higher than in AS, while in AS with lactic acid it was 100-times higher. Keywords: Ti6Al4V, SLM, corrosion, ion release, XPS, ToF-SIMS Published in DiRROS: 31.05.2023; Views: 478; Downloads: 370 Full text (15,86 MB) This document has many files! More... |
9. Water versus oil lubrication of laser-textured Ti6Al4V alloy upon addition of MoS2 nanotubes for green tribologyMarjetka Conradi, Bojan Podgornik, Aleksandra Kocijan, Maja Remškar, Damjan Klobčar, 2022, original scientific article Keywords: green tribology, surface texturing, MoS2 nanotubes, lubrication, Ti6Al4V alloy Published in DiRROS: 06.05.2022; Views: 650; Downloads: 206 Link to file |