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1.
Effect of deep cryogenic treatment on corrosion properties of various high-speed steels
Jure Voglar, Živa Novak, Patricia Jovičević Klug, Bojan Podgornik, Tadeja Kosec, 2021, izvirni znanstveni članek

Povzetek: The aim of the study was to evaluate the corrosion properties of three different grades of high-speed steel following a heat treatment procedure involving deep cryogenic treatment after quenching and to investigate how these properties are connected to the microstructure and hard- ness of the material. The hardness of steels was measured, and microstructural properties were determined through observation of the metallographically prepared steels using scanning electron microscopy. These studies were complemented corrosion evaluation by the use of corrosion potential measurement and linear polarization measurement of steels in a sodium tetraborate buffer at pH 10. The results showed that the deep cryogenic procedure of high-speed steel changed the microstructure and consequently affected the hardness of the investigated steels to different extents, depending on their chemical composition. Corrosion studies have confirmed that some high-speed steels have improved corrosion properties after deep cryogenic treatment. The most important improvement in corrosion resistance was observed for deep cryogenically treated high-speed steel EN 1.3395 (M3:2) by 31% when hardened to high hardness values and by 116% under lower hardness conditions. The test procedure for differentiating corrosion properties of differently heat-treated tool steels was established alongside the investigation.
Ključne besede: deep cryogenic treatment, corrosion, microstructure, hardness
Objavljeno v DiRROS: 01.08.2023; Ogledov: 277; Prenosov: 144
.pdf Celotno besedilo (5,82 MB)
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2.
Effect of the microstructural properties of copper on corrosion performance
Tadeja Kosec, Jure Voglar, Petra Močnik, Andraž Legat, 2021, izvirni znanstveni članek

Povzetek: The aim of the study was to define the influence of microstructural properties on the electrochemical properties of copper in four different forms: copper in sheet form, copper doped with phosphorus, electroplated copper and copper wire. Open circuit potential and polarization resistance measurements were carried out in order to determine the electrochemical properties and corrosion rates of copper in 0.1 M NaCl solution in oxic conditions at ambient temperature. Statistical evaluation of the electrochemical data was performed in order to differentiate between the various forms of copper samples. Microstructural and electrochemical investigations were combined with electron microscopy and Raman analysis of the corrosion products after immersion of the copper samples in a 0.1 M NaCl solution for 30 days. The various morphologies of copper corrosion products were identified and analyzed by Raman spectroscopy for the various forms of copper.
Ključne besede: copper, microstructura, corrosion, Raman
Objavljeno v DiRROS: 19.07.2023; Ogledov: 314; Prenosov: 149
.pdf Celotno besedilo (2,24 MB)
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