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Iskalni niz: "ključne besede" (microstructure) .

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Characterization of micro-threaded stem taper surface of cementless hip endoprostheses
Drago Dolinar, Boštjan Kocjančič, Klemen Avsec, Barbara Šetina, Aleksandra Kocijan, Matjaž Godec, Marko Sedlaček, Mojca Debeljak, John T. Grant, Timon Zupanc, Monika Jenko, 2024, izvirni znanstveni članek

Povzetek: We investigated micro-threaded stem taper surface and its impact on premature failures, aseptic loosening, and infection in cementless hip endoprostheses. Our study focused on the fretting, and crevice corrosion of micro-threaded tapers, as well as the characterization of the microstructure and surface properties of two new and three retrieved Zweymüller stem tapers. The retrieved samples were selected and examined based on the head–stem taper interface being the sole source of modularity with a metallic component, specifically between the Ti alloy taper stem and the ceramic head. To determine the surface chemistry and microstructures of both new and retrieved hip endoprostheses stem taper titanium alloy, scanning -electron microscopy (SEM) was employed for morphological and microstructural analyses. Energy dispersive spectroscopy (EDS) was utilized for characterizing chemical element distribution, and electron backscattered diffraction (EBSD) was used for phase analysis. The roughness of the micro-threated stem tapers from different manufacturers was investigated using an optical profilometer, with standard roughness parameters Ra (average surface roughness) and Rz (mean peak to valley height of the roughness profile) being measured. Electrochemical studies revealed no fretting corrosion in retrieved stem tapers with ceramic heads. Consequently, three retrieved tapers and two new ones for comparison underwent potentiodynamic measurements in Hank’s solution to determine the corrosion rate of new and retrieved stem taper surfaces. The results showed a low corrosion rate for both new and prematurely failed retrieved samples due to aseptic loosening. However, the corrosion rate was higher in infected and low-grade infected tapers. In conclusion, our study suggests that using ceramic heads reduces taper corrosion and subsequently decreases the incidence of premature failures in total hip arthroplasty.
Ključne besede: total hip arthroplasty, stem micro-threaded taper, taper surface morphology, microstructure, corrosion, Ti implant alloy
Objavljeno v DiRROS: 06.06.2024; Ogledov: 59; Prenosov: 49
.pdf Celotno besedilo (8,47 MB)
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Ingenious architecture and coloration generation in enamel of Rodent teeth
Vesna Šrot, Sophia Houari, Gregor Kapun, Birgit Bußmann, Felicitas Predel, Boštjan Pokorny, Elena Bužan, Ute Salzberger, Bernhard Fenk, Marion Kelsch, Peter van Aken, 2024, izvirni znanstveni članek

Povzetek: Teeth exemplify architectures comprising an interplay of inorganic and organic constituents, resulting in sophisticated natural composites. Rodents (Rodentia) showcase extraordinary adaptations, with their continuously growing incisors surpassing human teeth in functional and structural optimizations. In this study, employing state-of-the-art direct atomic-scale imaging and nanoscale spectroscopies, we present compelling evidence that the release of material from ameloblasts and the subsequent formation of iron-rich enamel and surface layers in the constantly growing incisors of rodents are complex orchestrated processes, intricately regulated and independent of environmental factors. The synergistic fusion of three-dimensional tomography and imaging techniques of etched rodent́s enamel unveils a direct correlation between the presence of pockets infused with ferrihydrite-like material and the acid resistant properties exhibited by the iron-rich enamel, fortifying it as an efficient protective shield. Moreover, observations using optical microscopy shed light on the role of iron-rich enamel as a microstructural element that acts as a path for color transmission, although the native color remains indistinguishable from that of regular enamel, challenging the prevailing paradigms. The redefinition of “pigmented enamel” to encompass ferrihydrite-like infusion in rodent incisors reshapes our perception of incisor microstructure and color generation. The functional significance of acid-resistant iron-rich enamel and the understanding of the underlying coloration mechanism in rodent incisors have far-reaching implications for human health, development of potentially groundbreaking dental materials, and restorative dentistry. These findings enable the creation of an entirely different class of dental biomaterials with enhanced properties, inspired by the ingenious designs found in nature.
Ključne besede: teeth microstructure, ameloblasts, ferritin, Fe-rich enamel, tomography, rodent
Objavljeno v DiRROS: 26.04.2024; Ogledov: 166; Prenosov: 164
.pdf Celotno besedilo (3,34 MB)
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Bioresorbability dependence on microstructure of additivelly- manufactured and conventionally-produced Fe-Mn alloys
Matjaž Godec, Jakob Kraner, Danijela Anica Skobir Balantič, Irena Paulin, Damjana Drobne, Veno Kononenko, Aleksandra Kocijan, Paul J. McGuiness, Črtomir Donik, 2024, zaključena znanstvena zbirka raziskovalnih podatkov

Povzetek: The dataset supports the results shown in the tables and figures in the article entitled “Bioresorbability Dependence on Microstructure of Additivelly-Manufactured and Conventionally-Produced Fe-Mn Alloys” (doi.org/10.1016/j.jmrt.2024.04.097). It contains measurements of corrosion resistance of Fe-Mn samples, phase analysis of samples A, B and C, surface and depth profiling XPS, EDS measurements of a cross-section of Fe-Mn powder particles and viability measurements results.
Ključne besede: Fe-Mn alloy, laser powder bed fusion, bioresorbable, microstructure, corrosion behaviour, biocompatibility
Objavljeno v DiRROS: 12.04.2024; Ogledov: 288; Prenosov: 151
.xlsx Celotno besedilo (2,55 MB)
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The effect of heat treatment on the interface of 155 PH martensitic stainless steel and SAF 2507 duplex steel in functionally graded AM components
Martina Koukolíková, Pavel Podaný, Sylwia Rzepa, Michal Brázda, Aleksandra Kocijan, 2023, izvirni znanstveni članek

Povzetek: Multi-material components, also known as functionally graded materials (FGMs), are innovative materials that possess unique properties due to their composition and have many potential applications in engineering and science. The effect of the heat treatment (HT) of functionally graded materials 15–5 precipitation-hardened (PH) martensitic steel and SAF 2507 duplex stainless steel (and the opposite order of deposition, i.e. SAF 2507 first followed by 15–5 PH stainless steel) on the interface microstructures was systematically investigated in the presented research. The choice of HT followed the trend of optimum post-processing for the individual alloys. A significant modification in the interface microstructure, characterized in the microstructural transition zone (MTZ) formed above the fusion line. Mechanical properties by miniaturized testing method including hardness measurement characterized both types of interfaces. The sequence of the materials’ application did not have a significant effect on their final mechanical tensile properties in the heat-treated states. Nevertheless, the microstructural change at the MTZ led to drop in the hardness at the interface. The research presents heat-treated FGMs in a horizontal configuration to form a high-quality metallurgical joint between heterogeneous materials manufactured by powder-based directed energy deposition method.
Ključne besede: heat treatment, additive manufacturing, martensitic stainless steel, duplex steel, microstructure, mechanical properties
Objavljeno v DiRROS: 04.04.2024; Ogledov: 198; Prenosov: 40
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