1. Harmonizing microstructures and enhancing mechanical resilience : novel powder metallurgy approach for Zn–Mg alloysAnna Boukalová, Jiří Kubásek, David Nečas, Peter Minárik, Črtomir Donik, Drahomír Dvorský, Dalibor Vojtěch, Alena Michalcová, Matjaž Godec, Irena Paulin, 2024, izvirni znanstveni članek Povzetek: Zinc alloys are recognised for their excellent biocompatibility and favourable corrosion rates, making them suitable for bioabsorbable implants. However, their mechanical properties necessitate improvement to fulfil the rigorous requirements of biomedical applications. This research focuses on engineering pseudo-harmonic structures within zinc alloys through a comprehensive method combining mechanical alloying, spark plasma sintering, and hot extrusion techniques. This fabrication process results in a composite material characterised by a soft core surrounded by a continuous, three-dimensional, ultrafine-grained hard shell. The experiment involved blending pure zinc with Zn–1Mg alloy powder, leading to the formation of both ductile zinc and fine-grained Zn–1Mg regions. While the Mg2Zn11 intermetallic phase was found to enhance the alloy's mechanical strength, the presence of oxide shells adversely affected the material's properties. The elimination of these shells via hot extrusion markedly improved the alloy's tensile strength, reaching an average value of tensile strength of 333 ± 7 MPa. This study provides significant insights into the material engineering of zinc-based alloys for biodegradable implant applications, demonstrating a viable approach to optimising their mechanical performance. Ključne besede: zinc, magnesium, biodegradable, powder metallurgy, harmonic structure Objavljeno v DiRROS: 23.07.2024; Ogledov: 191; Prenosov: 170 Celotno besedilo (14,29 MB) Gradivo ima več datotek! Več... |
2. Microstructural, corrosion and mechanical properties of a WE43 alloy : conventional extrusion versus SPDAnna Dobkowska, Aleksandra Zielińska, Irena Paulin, Črtomir Donik, Milena Koralnik, Bogusława Adamczyk-Cieślak, Monika Wieczorek-Czarnocka, Dariusz Kuc, Jiří Kubásek, Tomasz Mikuszewski, Matjaž Godec, Jarosław Mizera, 2024, izvirni znanstveni članek Povzetek: A hexagonal close-packed-structure WE43 alloy was extruded without any preheating of the initial billet using extrusion with an oscillating die to improve the corrosion and mechanical properties. The WE43 alloy was extruded at high ratios of R 1 5:1, R 2 7:1 and R 3 10:1. Electron back-scatter diffraction and transmission electron microscopy were used to determine the microstructural properties of the alloys. The influence of the extrusion method and the extrusion ratios on the corrosion and mechanical properties were investigated. Electrochemical tests were performed, and the corrosion damage was inspected. Tensile tests were made using micro specimens. When compared to conventional extrusion, the microstructural changes obtained with the KoBo method at R 5:1 increased the corrosion resistance, which was not only due to the grain refinement, but also due to the intensity of the texture. A decline in the corrosion resistance of the alloys deformed at higher extrusion ratios was observed. This was a result of the massive plastic strain imposed by the KoBo die. The room-temperature mechanical properties of the KoBo-extruded alloys were improved. However, at higher temperatures the mechanical properties decreased due to the solutioning of tiny triple precipitates. Ključne besede: WE43, several plastic deformation, microstructure, corrosion, mechanical properties Objavljeno v DiRROS: 23.07.2024; Ogledov: 202; Prenosov: 60 Povezava na datoteko |
3. Characterization of micro-threaded stem taper surface of cementless hip endoprosthesesDrago Dolinar, Boštjan Kocjančič, Klemen Avsec, Barbara Šetina, Aleksandra Kocijan, Matjaž Godec, Marko Sedlaček, Mojca Debeljak, John T. Grant, Timon Zupanc, Monika Jenko, 2024, izvirni znanstveni članek Povzetek: We investigated micro-threaded stem taper surface and its impact on premature failures, aseptic loosening, and infection in cementless hip endoprostheses. Our study focused on the fretting, and crevice corrosion of micro-threaded tapers, as well as the characterization of the microstructure and surface properties of two new and three retrieved Zweymüller stem tapers. The retrieved samples were selected and examined based on the head–stem taper interface being the sole source of modularity with a metallic component, specifically between the Ti alloy taper stem and the ceramic head. To determine the surface chemistry and microstructures of both new and retrieved hip endoprostheses stem taper titanium alloy, scanning -electron microscopy (SEM) was employed for morphological and microstructural analyses. Energy dispersive spectroscopy (EDS) was utilized for characterizing chemical element distribution, and electron backscattered diffraction (EBSD) was used for phase analysis. The roughness of the micro-threated stem tapers from different manufacturers was investigated using an optical profilometer, with standard roughness parameters Ra (average surface roughness) and Rz (mean peak to valley height of the roughness profile) being measured. Electrochemical studies revealed no fretting corrosion in retrieved stem tapers with ceramic heads. Consequently, three retrieved tapers and two new ones for comparison underwent potentiodynamic measurements in Hank’s solution to determine the corrosion rate of new and retrieved stem taper surfaces. The results showed a low corrosion rate for both new and prematurely failed retrieved samples due to aseptic loosening. However, the corrosion rate was higher in infected and low-grade infected tapers. In conclusion, our study suggests that using ceramic heads reduces taper corrosion and subsequently decreases the incidence of premature failures in total hip arthroplasty. Ključne besede: total hip arthroplasty, stem micro-threaded taper, taper surface morphology, microstructure, corrosion, Ti implant alloy Objavljeno v DiRROS: 06.06.2024; Ogledov: 270; Prenosov: 235 Celotno besedilo (8,47 MB) Gradivo ima več datotek! Več... |
4. Microstructure and properties of an AZ61 alloy after extrusion with a forward-backward oscillating die without preheating of the initial billetAnna Dobkowska, Aleksandra Zielińska, Irena Paulin, Črtomir Donik, Maciej Łojkowski, Milena Koralnik, Bogusława Adamczyk-Cieślak, Krystian Paradowski, Marek Tkocz, Dariusz Kuc, Jiří Kubásek, Matjaž Godec, Wojciech Święszkowski, 2023, izvirni znanstveni članek Ključne besede: magnesium alloys, severe plastic deformation, microstructure, mechanical properties, corrosion, extrusion, high deformation ratio Objavljeno v DiRROS: 17.05.2024; Ogledov: 384; Prenosov: 203 Povezava na datoteko |
5. Bioresorbability dependence on microstructure of additivelly- manufactured and conventionally-produced Fe-Mn alloysMatjaž Godec, Jakob Kraner, Danijela Anica Skobir Balantič, Irena Paulin, Damjana Drobne, Veno Kononenko, Aleksandra Kocijan, Paul J. McGuiness, Črtomir Donik, 2024, izvirni znanstveni članek Ključne besede: Fe-Mn alloy, laser powder bed fusion, bioresorbable, microstructure, corrosion behaviour, biocompatibility Objavljeno v DiRROS: 06.05.2024; Ogledov: 409; Prenosov: 306 Celotno besedilo (12,78 MB) Gradivo ima več datotek! Več... |
6. Bioresorbability dependence on microstructure of additivelly- manufactured and conventionally-produced Fe-Mn alloysMatjaž Godec, Jakob Kraner, Danijela Anica Skobir Balantič, Irena Paulin, Damjana Drobne, Veno Kononenko, Aleksandra Kocijan, Paul J. McGuiness, Črtomir Donik, 2024, zaključena znanstvena zbirka raziskovalnih podatkov Povzetek: The dataset supports the results shown in the tables and figures in the article entitled “Bioresorbability Dependence on Microstructure of Additivelly-Manufactured and Conventionally-Produced Fe-Mn Alloys” (doi.org/10.1016/j.jmrt.2024.04.097). It contains measurements of corrosion resistance of Fe-Mn samples, phase analysis of samples A, B and C, surface and depth profiling XPS, EDS measurements of a cross-section of Fe-Mn powder particles and viability measurements results. Ključne besede: Fe-Mn alloy, laser powder bed fusion, bioresorbable, microstructure, corrosion behaviour, biocompatibility Objavljeno v DiRROS: 12.04.2024; Ogledov: 557; Prenosov: 374 Celotno besedilo (2,55 MB) Gradivo ima več datotek! Več... |
7. A coupled convective-diffusive model of heat transfer and melt-pool dynamics in additive manufacturingTijan Mede, Matjaž Godec, 2024, elaborat, predštudija, študija Ključne besede: additive manufacturing, selective laser melting, laser powder-bed fusion, melt-pool, heat transfer, convection Objavljeno v DiRROS: 05.04.2024; Ogledov: 409; Prenosov: 0 |
8. Effect of post-treated low-temperature plasma nitriding on the wear and corrosion resistance of 316L stainless steel manufactured by laser powder-bed fusionMatjaž Godec, Črtomir Donik, Aleksandra Kocijan, Bojan Podgornik, Danijela Anica Skobir Balantič, 2020, izvirni znanstveni članek Ključne besede: austenitic stainless steel, powder bed fusion, low-temperature plasma nitriding, wear and corrosion behaviour, dislocation cell structure Objavljeno v DiRROS: 25.03.2024; Ogledov: 380; Prenosov: 235 Celotno besedilo (3,28 MB) Gradivo ima več datotek! Več... |
9. Use of plasma nitriding to improve the wear and corrosion resistance of 18Ni-300 maraging steel manufactured by selective laser meltingMatjaž Godec, Bojan Podgornik, Aleksandra Kocijan, Črtomir Donik, Danijela Anica Skobir Balantič, 2021, izvirni znanstveni članek Ključne besede: selective laser melting, 18Ni-300 maraging steel, heat treatment, plasma nitriding, retained and reverted austenite, wear and corrosion behaviour Objavljeno v DiRROS: 25.03.2024; Ogledov: 411; Prenosov: 187 Celotno besedilo (3,37 MB) Gradivo ima več datotek! Več... |
10. Evolution of microstructure and embrittlement during the tempering process in SiCrCu medium-carbon steelsPavel Salvetr, Aleksandr Gokhman, Črtomir Donik, Zbyšek Nový, Jakub Kotous, Matjaž Godec, 2023, izvirni znanstveni članek Ključne besede: medium-carbon steel, tempering martensite embrittlement, microstructure, mechanical properties Objavljeno v DiRROS: 08.03.2024; Ogledov: 353; Prenosov: 229 Celotno besedilo (4,44 MB) Gradivo ima več datotek! Več... |